초록문의 abstract@kcsnet.or.kr

결제문의 member@kcsnet.or.kr

현재 가능한 작업은 아래와 같습니다.
  • 02월 19일 10시 이후 : 초록수정 불가능, 일정확인 및 검색만 가능

제121회 대한화학회 학술발표회, 총회 및 기기전시회 안내 A study on the determination of inorganic selenium by solid phase extraction and laser induced breakdown spectroscopy

2018년 2월 6일 14시 10분 45초
ANAL1.O-7 이곳을 클릭하시면 발표코드에 대한 설명을 보실 수 있습니다.
목 10시 : 07분
Analytical Chemistry - Oral Presentation of Young Analytical Chemists I
저자 및
Seon Hwa Lee
Department of Chemistry, Mokpo National University, Korea
The toxicity and chemical properties of selenium depend on the concentration and the chemical structure present in the natural environment. Inorganic selenium is more toxic than organic selenium, thus the accurate determination of inorganic selenium in various samples is needed. HG-AAS(Hydride Generation Atomic Absorption Spectroscopy), HPLC-ICP-MS(High Performance Liquid Chromatography-Inductively Coupled Plasma-Mass Spectrometry) and GC-MS(Gas Chromatograph-Mass Spectrometry) are the current of methods for the determination of inorganic selenium. However, these methods have the disadvantage of expensive equipment, complicated sample preparation and long analysis time. A new analytical method was developed using the SPE membrane filter with LIBS for the determination of inorganic selenium species. The detection limit of inorganic selenium by the new analytical method was 11.21 mg / kg, and the recoveries of Se (Ⅵ) 98.5 ± 5.31% and 101.80 ± 2.01%, respectively. This new speciation method is cost effective, simple and not labor intensive for the quantitation of inorganic selenium.