123rd General Meeting of the KCS

Type Poster Presentation
Area Analytical Chemistry
Room No. Exhibition Hall 2
Time 4월 19일 (금요일) 11:00~12:30
Code ANAL.P-242
Subject Enantioseparation on 3,5-dinitrobenzoyl amino alcohol derived CSPs by high performance liquid chromatography and supercritical fluid chromatography.
Authors Gyuri Kim, Heo KyuSung, Jae Jeong Ryoo1,*
Department of Chemistry, Kyungpook National University, Korea
1Department of Chemical Education, Kyungpook National University, Korea
Abstract

N-3,5-Dinitrobenzoyl(DNB) phenylglycinol derived CSP(CSP 1) and leucinol derived CSP(CSP 2) were used for the separation of various chiral analytes.1,2 In this study, we synthesized the chiral stationary phases using 2 ㎛ silica gel instead of 5 ㎛ silica gel to improve the number of theoretical plate and use for supercritical fluid chromatography, compared the resolution. 1. J. J. Yu; D. H. Ryoo; J. M. Lee; J. J. Ryoo. Chirality 2016, 28, 186. 2. J. J. Ryoo; T. H. Kim; S. H. Im; Y. H. Jeong; J. Y. Park; S. H. Choi; K. P. Lee; J. H. Park. J. Chromatogr. A 2003, 987, 429.

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